Instrumental Data for Drug Analysis - 6 Volume Set

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Instrumental Data for Drug Analysis

The authors and publisher have made every effort to assure the accuracy of the information in this book; however, they cannot be responsible for errors in publication or for any consequences arising from the use of the data published in INSTRUMENTAL DATA FOR DRUG ANALYSIS, THIRD EDITION.

Instrumental Data for Drug Analysis Third Edition Volume 4 Terry Mills III, James Conrad Roberson, Christian C. Matchett, Mathew J. Simon, Mark D. Burns, and Robert J. Ollis Jr.

Boca Raton London New York

A CRC title, part of the Taylor & Francis imprint, a member of the Taylor & Francis Group, the academic division of T&F Informa plc.

Published in 2006 by CRC Press Taylor & Francis Group 6000 Broken Sound Parkway NW, Suite 300 Boca Raton, FL 33487-2742 © 2006 by Taylor & Francis Group, LLC CRC Press is an imprint of Taylor & Francis Group No claim to original U.S. Government works Printed in the United States of America on acid-free paper 10 9 8 7 6 5 4 3 2 1 International Standard Book Number-10: 0-8493-1974-9 (Hardcover) International Standard Book Number-13: 978-0-8493-1974-7 (Hardcover) Library of Congress Card Number 2005048542 This book contains information obtained from authentic and highly regarded sources. Reprinted material is quoted with permission, and sources are indicated. A wide variety of references are listed. Reasonable efforts have been made to publish reliable data and information, but the author and the publisher cannot assume responsibility for the validity of all materials or for the consequences of their use. No part of this book may be reprinted, reproduced, transmitted, or utilized in any form by any electronic, mechanical, or other means, now known or hereafter invented, including photocopying, microfilming, and recording, or in any information storage or retrieval system, without written permission from the publishers. For permission to photocopy or use material electronically from this work, please access www.copyright.com (http://www.copyright.com/) or contact the Copyright Clearance Center, Inc. (CCC) 222 Rosewood Drive, Danvers, MA 01923, 978-750-8400. CCC is a not-for-profit organization that provides licenses and registration for a variety of users. For organizations that have been granted a photocopy license by the CCC, a separate system of payment has been arranged. Trademark Notice: Product or corporate names may be trademarks or registered trademarks, and are used only for identification and explanation without intent to infringe. Library of Congress Cataloging-in-Publication Data Instrumental data for drug analysis / by Terry Mills, III … [et al.]. – 3rd ed. p. cm. Includes index. Previous ed.: Instrumental data for drug analysis / by Terry Mills. Boca Raton : CRC Press 1993-1996. ISBN 0-8493-1974-9 (alk. paper) Drugs – Analysis – Standards. 2. Drugs – Spectra – Standards. 3. Instrumental analysis – Standards. I. Mills, Terry. II. Mills, Terry. Instrumental data for drug analysis. RS189.M54 2005 615’.1901 – dc22

2005048542

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Table of Contents VOLUME 1 PREFACE ................................................................................................................................................................vii ACKNOWLEDGMENTS.........................................................................................................................................ix INTRODUCTION ................................................................................................................................................... xi DRUG DATA Acebutolol – Dapsone .........................................................................................................................2

VOLUME 2 DRUG DATA Dauromycin – Indigotin Disulfonate...........................................................................................................816

VOLUME 3 DRUG DATA Indole-3-Acetic Acid – Phendimetrazine ..................................................................................................1638

VOLUME 4 DRUG DATA Phenelzine – Zoxazolamine .......................................................................................................................2454

VOLUME 5 RAMAN SPECTRA DATA ................................................................................................................................3279 MASS SPECTRA OF PESTICIDES ..................................................................................................................3691 MASS SPECTRA OF DERIVATIZED DRUGS................................................................................................3803 GAS CHROMATOGRAPHY/INFRARED SPECTRA OF DRUGS.................................................................3949

VOLUME 6 APPENDIX A: Standard KBr Infrared Spectra and Standard NMR Solvent Spectra ......................................4177 APPENDIX B: Supplemental Infrared Spectra ..................................................................................................4185 APPENDIX C: Supplemental NMR Spectra......................................................................................................4267 APPENDIX D: Ultraviolet Absorption Maxima ................................................................................................4293 APPENDIX E: Infrared Index.............................................................................................................................4371 APPENDIX F: Mass Spectra Indices of Drugs..................................................................................................4409 APPENDIX G: Mass Spectra Indices of Pesticides ...........................................................................................4461 APPENDIX H: Molecular Formula Index..........................................................................................................4473 APPENDIX I: Gas Chromatographic Data .......................................................................................................4509 INDEX TO SPECIFIC COMPOUNDS ..............................................................................................................4529

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2921

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2925

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2927

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2957

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2959

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2961

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2963

2964

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2965

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2967

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2969

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2971

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2973

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2975

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2977

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2979

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2981

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2983

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2985

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2987

2988

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2989

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2991

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2993

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2995

2996

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2997

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2999

3000

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

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3004

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3015

3016

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3017

3018

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3019

3020

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3021

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3035

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3037

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3039

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3041

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3043

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3045

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3047

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3049

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3051

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3053

3054

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3055

3056

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3057

3058

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3059

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3075

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3077

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3081

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3083

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3085

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3091

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3095

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3097

3098

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3099

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3101

3102

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3103

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3105

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3107

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3109

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3111

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3113

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3115

3116

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3117

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3119

3120

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3121

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3123

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3125

3126

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3127

3128

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3129

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3131

3132

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3133

3134

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3135

3136

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3137

3138

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3139

3140

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3141

3142

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3143

3144

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3145

3146

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3147

3148

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3149

3150

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3151

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3153

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3155

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3157

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3159

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3163

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3165

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3167

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3169

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3171

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3173

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3175

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3177

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3179

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3181

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3183

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3185

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3189

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3191

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3193

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3195

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3197

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3199

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3201

3202

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3203

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3205

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3207

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3209

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3211

3212

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3213

3214

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3215

3216

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3217

3218

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3219

3220

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3221

3222

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3223

3224

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3225

3226

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3227

3228

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3229

3230

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3231

3232

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3233

3234

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3235

3236

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3237

3238

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3239

3240

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3241

3242

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3243

3244

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3245

3246

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3247

3248

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3249

3250

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3251

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3253

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3255

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3257

3258

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3259

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3261

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3263

3264

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3265

3266

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3267

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3269

3270

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3271

3272

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3273

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3275

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Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3277